Information card for entry 4318578

Structure parameters

• Common name: complex 5, Nd(tBuMeMe)3
• Formula: C33 H60 N3 Nd O6
• Calculated formula: C33 H60 N3 Nd O6
• Title of publication: Synthesis and Characterization of Volatile, Fluorine-Free β-Ketoiminate Lanthanide MOCVD Precursors and Their Implementation in Low-Temperature Growth of Epitaxial CeO2 Buffer Layers for Superconducting Electronics
• Authors of publication: Nikki L. Edleman; Anchuan Wang; John A. Belot; Andrew W. Metz; Jason R. Babcock; Amber M. Kawaoka; Jun Ni; Matthew V. Metz; Christine J. Flaschenriem; Charlotte L. Stern; Louise M. Liable-Sands; Arnold L. Rheingold; Paul R. Markworth; Robert P. H. Chang; Michael P. Chudzik; Carl R. Kannewurf; Tobin J. Marks
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 5005 - 5023
• a: 13.3606 ± 0.0002 Å
• b: 17.1475 ± 0.0002 Å
• c: 16.4002 ± 0.0002 Å
• α: 90°
• β: 98.9027 ± 0.0007°
• γ: 90°
• Cell volume: 3712.03 ± 0.08 ų
• Cell temperature: 198 ± 2 K
• Ambient diffraction temperature: 198 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1159
• Residual factor for significantly intense reflections: 0.0851
• Weighted residual factors for all reflections: 0.2713
• Weighted residual factors for significantly intense reflections: 0.2306
• Goodness-of-fit parameter for all reflections: 1.667
• Goodness-of-fit parameter for significantly intense reflections: 1.741
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No