Information card for entry 4318606

Structure parameters

• Formula: C52 H62 F6 N3 O4 P3 Rh
• Calculated formula: C52 H62 F6 N3 O4 P3 Rh
• Title of publication: Rhodium(I) and Rhodium(III) Complexes Containing the Chiral Ligand 2,6-Bis[4'(S)-isopropyloxazolin-2'-yl]pyridine (Pybox): An Unprecedented Monohapto Coordination of Pybox
• Authors of publication: Darío Cuervo; Josefina Díez; M. Pilar Gamasa; S. García-Granda; José Gimeno
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4999 - 5001
• a: 9.5651 ± 0.0003 Å
• b: 24.1074 ± 0.0007 Å
• c: 11.4952 ± 0.0004 Å
• α: 90°
• β: 90.9181 ± 0.0014°
• γ: 90°
• Cell volume: 2650.33 ± 0.15 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 200 ± 2 K
• Number of distinct elements: 7
• Space group number: 4
• Hermann-Mauguin space group symbol: P 1 21 1
• Hall space group symbol: P 2yb
• Residual factor for all reflections: 0.0788
• Residual factor for significantly intense reflections: 0.0662
• Weighted residual factors for significantly intense reflections: 0.1689
• Weighted residual factors for all reflections included in the refinement: 0.1814
• Goodness-of-fit parameter for all reflections included in the refinement: 1.064
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No