Information card for entry 4318644

Structure parameters

• Common name: Lead tetrakis(imidazolyl)borate nitrate
• Formula: C12 H14.65 B N9 O4.32 Pb
• Calculated formula: C12 H14.646 B N9 O4.323 Pb
• Title of publication: Construction of a Functional Layered Solid Using the Tetrakis(imidazolyl)borate Coordinating Anion
• Authors of publication: Barton H. Hamilton; Kathryn A. Kelly; Todd A. Wagler; Matthew P. Espe; Christopher J. Ziegler
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 4984 - 4986
• a: 8.5337 ± 0.0008 Å
• b: 10.7463 ± 0.0009 Å
• c: 11.2476 ± 0.001 Å
• α: 74.684 ± 0.001°
• β: 79.284 ± 0.001°
• γ: 67.012 ± 0.001°
• Cell volume: 911.84 ± 0.14 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0371
• Residual factor for significantly intense reflections: 0.0316
• Weighted residual factors for significantly intense reflections: 0.0702
• Weighted residual factors for all reflections included in the refinement: 0.0721
• Goodness-of-fit parameter for all reflections included in the refinement: 1.075
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No