Information card for entry 4318662

Structure parameters

• Formula: C18 H19 Co N4 O3 S4
• Calculated formula: C18 H19 Co N4 O3 S4
• Title of publication: Oxovanadium(V) and Cobalt(III) Complexes of Dithiocarbazate-Based Schiff Base Ligands: Formation of a Thiadiazole Ring by Vanadium-Induced Cyclization of the Coordinated Ligand
• Authors of publication: Subodh Kanti Dutta; Satyabrata Samanta; Dipesh Ghosh; Ray J. Butcher; Muktimoy Chaudhury
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 5555 - 5560
• a: 12.0842 ± 0.0008 Å
• b: 13.5251 ± 0.0009 Å
• c: 14.196 ± 0.001 Å
• α: 78.122 ± 0.006°
• β: 73.888 ± 0.006°
• γ: 78.255 ± 0.006°
• Cell volume: 2154.7 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0512
• Residual factor for significantly intense reflections: 0.0343
• Weighted residual factors for significantly intense reflections: 0.0794
• Weighted residual factors for all reflections included in the refinement: 0.0873
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No