Information card for entry 4318713

Structure parameters

• Formula: C54 H65 F Li N3 O7 Rh3
• Calculated formula: C54 H65 F Li N3 O7 Rh3
• Title of publication: Stabilization of Molecular LiF and LiFHF inside Metallamacrocyclic Hosts
• Authors of publication: Marie-Line Lehaire; Rosario Scopelliti; Kay Severin
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 5466 - 5474
• a: 44.177 ± 0.009 Å
• b: 12.39 ± 0.003 Å
• c: 20.164 ± 0.004 Å
• α: 90°
• β: 112.44 ± 0.03°
• γ: 90°
• Cell volume: 10201 ± 4 ų
• Cell temperature: 143 ± 2 K
• Ambient diffraction temperature: 143 ± 2 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.0512
• Residual factor for significantly intense reflections: 0.0469
• Weighted residual factors for significantly intense reflections: 0.1256
• Weighted residual factors for all reflections included in the refinement: 0.1284
• Goodness-of-fit parameter for all reflections included in the refinement: 1.041
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No