Information card for entry 4318736

Structure parameters

• Formula: C73 H84 B Cl2 F4 N2 O2 P2 Rh S2 Zn
• Calculated formula: C70 H68 B F4 N2 O2 P2 Rh S2 Zn
• Title of publication: A Tetranuclear Heterobimetallic Square Formed from the Cooperative Ligand Binding Properties of Square Planar and Tetrahedral Metal Centers
• Authors of publication: Nathan C. Gianneschi; Chad A. Mirkin; Lev N. Zakharov; Arnold L. Rheingold
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 5326 - 5328
• a: 13.0662 ± 0.0008 Å
• b: 17.7855 ± 0.001 Å
• c: 18.327 ± 0.0011 Å
• α: 105.105 ± 0.001°
• β: 95.586 ± 0.001°
• γ: 105.462 ± 0.001°
• Cell volume: 3898.8 ± 0.4 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 11
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1292
• Residual factor for significantly intense reflections: 0.0903
• Weighted residual factors for significantly intense reflections: 0.2092
• Weighted residual factors for all reflections included in the refinement: 0.2256
• Goodness-of-fit parameter for all reflections included in the refinement: 1.059
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No