Information card for entry 4318807

Structure parameters

• Formula: C12 H29 F2 N3 Si
• Calculated formula: C12 H29 F2 N3 Si
• Title of publication: Hexaalkylguanidinium and 2-(Dialkylamino)-1,3-dimethylimidazolinium Trimethyldifluorosiliconates and Perfluoroalkoxides. Accidental Isolation and Molecular Structure of [C(NMe2)3]+F-.6CH2Cl2
• Authors of publication: Alexander A. Kolomeitsev; German Bissky; Jan Barten; Natalya Kalinovich; Enno Lork; Gerd-Volker Röschenthaler
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 6118 - 6124
• a: 9.135 ± 0.002 Å
• b: 8.6 ± 0.002 Å
• c: 10.58 ± 0.002 Å
• α: 90°
• β: 96.99 ± 0.03°
• γ: 90°
• Cell volume: 825 ± 0.3 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0657
• Residual factor for significantly intense reflections: 0.0496
• Weighted residual factors for significantly intense reflections: 0.1377
• Weighted residual factors for all reflections included in the refinement: 0.1456
• Goodness-of-fit parameter for all reflections included in the refinement: 1.07
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No