Information card for entry 4318810

Structure parameters

• Formula: C15 H20 N2 O11 Pb2
• Calculated formula: C15 H14 N2 O11 Pb2
• Title of publication: Holo- and Hemidirected Lead(II) in the Polymeric [Pb4(μ-3,4-TDTA)2(H2O)2].4H2O Complex. N,N,N',N'-Tetraacetate Ligands Derived fromo-Phenylenediamines as Sequestering Agents for Lead(II)
• Authors of publication: Joaquín Sanchiz; Pedro Esparza; Diego Villagra; Sixto Domínguez; Alfredo Mederos; Felipe Brito; Lorena Araujo; Agustin Sánchez; Juan Manuel Arrieta
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 6048 - 6055
• a: 8.911 ± 0.003 Å
• b: 9.601 ± 0.002 Å
• c: 13.052 ± 0.002 Å
• α: 74.41 ± 0.01°
• β: 75.26 ± 0.02°
• γ: 69.61 ± 0.02°
• Cell volume: 992.1 ± 0.4 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.04
• Residual factor for significantly intense reflections: 0.0319
• Weighted residual factors for significantly intense reflections: 0.0803
• Weighted residual factors for all reflections included in the refinement: 0.0839
• Goodness-of-fit parameter for all reflections included in the refinement: 1.052
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No