Information card for entry 4318891

Structure parameters

• Formula: C30 H34 Cl2 F6 N8 P Rh
• Calculated formula: C30 H30 Cl2 F6 N8 P Rh
• SMILES: [P](F)(F)(F)(F)(F)[F-].CC#N.Cl[Rh]123([N](CC[N]1(Cc1cccc[n]31)Cc1ccccn1)(Cc1cccc[n]21)Cc1ccccn1)Cl.CC#N
• Title of publication: N,N,N',N'-Tetrakis(2-pyridylmethyl)ethylenediamine and Its Analogues as Hypodentate Ligands. Synthesis and Characterization of the Rhodium(III), Ruthenium(II), and Palladium(II) Complexes
• Authors of publication: Maxim Sokolov; Keisuke Umakoshi; Yoichi Sasaki
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 6237 - 6243
• a: 16.974 ± 0.004 Å
• b: 8.064 ± 0.003 Å
• c: 13.247 ± 0.003 Å
• α: 90°
• β: 106.37 ± 0.02°
• γ: 90°
• Cell volume: 1739.7 ± 0.9 ų
• Cell temperature: 296.2 K
• Number of distinct elements: 7
• Space group number: 5
• Hermann-Mauguin space group symbol: C 1 2 1
• Hall space group symbol: C 2y
• Residual factor for significantly intense reflections: 0.0537
• Weighted residual factors for all reflections included in the refinement: 0.087
• Goodness-of-fit parameter for all reflections included in the refinement: 1.165
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoK$B-B(J
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No