Information card for entry 4319013

Structure parameters

• Formula: C22 H39 Li2 N2 O2 P S
• Calculated formula: C22 H39 Li2 N2 O2 P S
• Title of publication: Synthesis and X-ray Structures of Dilithium Complexes of the Phosphonate Anions [PhP(E)(NtBu)2]2- (E = O, S, Se, Te) and Dimethylaluminum Derivatives of [PhP(E)(NtBu)(NHtBu)]- (E = S, Se)
• Authors of publication: Glen G. Briand; Tristram Chivers; Mark Krahn; Masood Parvez
• Journal of publication: Inorganic Chemistry
• Year of publication: 2002
• Journal volume: 41
• Pages of publication: 6808 - 6815
• a: 9.7079 ± 0.0001 Å
• b: 28.825 ± 0.0004 Å
• c: 10.3105 ± 0.0002 Å
• α: 90°
• β: 115.314 ± 0.0006°
• γ: 90°
• Cell volume: 2608.15 ± 0.07 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0816
• Residual factor for significantly intense reflections: 0.0508
• Weighted residual factors for significantly intense reflections: 0.1197
• Weighted residual factors for all reflections included in the refinement: 0.1371
• Goodness-of-fit parameter for all reflections included in the refinement: 0.969
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No