Information card for entry 4319112

Structure parameters

• Formula: C66 H60 Ho2 N10 Te2
• Calculated formula: C66 H60 Ho2 N10 Te2
• Title of publication: Heteroleptic Lanthanide Compounds with Chalcogenolate Ligands: Reduction of PhNNPh/PhEEPh (E = Se or Te) Mixtures with Ln (Ln = Ho, Er, Tm, Yb). Thermolysis Can Give LnN or LnE
• Authors of publication: Anna Kornienko; Deborah Freedman; Thomas J. Emge; John G. Brennan
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 140 - 145
• a: 10.349 ± 0.002 Å
• b: 17.662 ± 0.004 Å
• c: 17.73 ± 0.008 Å
• α: 75.82 ± 0.03°
• β: 74.11 ± 0.03°
• γ: 89.45 ± 0.02°
• Cell volume: 3016.2 ± 1.8 ų
• Cell temperature: 153 ± 5 K
• Ambient diffraction temperature: 153 ± 5 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0651
• Residual factor for significantly intense reflections: 0.0323
• Weighted residual factors for significantly intense reflections: 0.0693
• Weighted residual factors for all reflections included in the refinement: 0.074
• Goodness-of-fit parameter for all reflections included in the refinement: 0.998
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No