Information card for entry 4319155

Structure parameters

• Formula: C45 H39 Cl4 N3 O P2 Re
• Calculated formula: C45 H39 Cl4 N3 O P2 Re
• Title of publication: Oxygen Atom Transfer from Nitrogenous ReVO Reagents to Diphosphines and Subsequent Transformations. Rhenium(III) Products and Reaction Models
• Authors of publication: Sibaprasad Bhattacharyya; Indranil Chakraborty; Bimal Kumar Dirghangi; Animesh Chakravorty
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 286 - 293
• a: 10.034 ± 0.002 Å
• b: 10.737 ± 0.002 Å
• c: 20.357 ± 0.004 Å
• α: 89.38 ± 0.03°
• β: 87.79 ± 0.03°
• γ: 80.22 ± 0.03°
• Cell volume: 2159.7 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0421
• Residual factor for significantly intense reflections: 0.0303
• Weighted residual factors for all reflections: 0.082
• Weighted residual factors for significantly intense reflections: 0.069
• Goodness-of-fit parameter for all reflections: 1.044
• Goodness-of-fit parameter for significantly intense reflections: 1.037
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No