Information card for entry 4319230

Structure parameters

• Formula: C44 H74 In2 Ni4 O4 Si6
• Calculated formula: C44 H74 In2 Ni4 O4 Si6
• Title of publication: Reaction of Ni2Cp2(μ-CO)2 with the Alkylgallium(I) and Alkylindium(I) Compounds E4[C(SiMe3)3]4 (E = Ga, In). Insertion of E-R Groups into the Ni-Ni Bond versus Replacement of CO by the Isolobal E-R Ligands
• Authors of publication: Werner Uhl; Sandra Melle; Gernot Frenking; Michael Hartmann
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 750 - 755
• a: 9.393 ± 0.001 Å
• b: 15.856 ± 0.002 Å
• c: 19.268 ± 0.003 Å
• α: 84.6 ± 0.02°
• β: 89.36 ± 0.03°
• γ: 89.31 ± 0.03°
• Cell volume: 2856.6 ± 0.7 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0497
• Residual factor for significantly intense reflections: 0.0403
• Weighted residual factors for all reflections: 0.0769
• Weighted residual factors for significantly intense reflections: 0.075
• Goodness-of-fit parameter for all reflections: 2.827
• Goodness-of-fit parameter for significantly intense reflections: 2.987
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No