Information card for entry 4319292

Structure parameters

• Formula: C93.75 H129.75 Cl27.25 O6 P2 Pd2
• Calculated formula: C90.5 H126.5 Cl17.5 O6 P2 Pd2
• Title of publication: Sterically Crowded, Rigid,C3 Symmetric Phosphites: Synthesis, Structure, and Preparation of Metal Complexes
• Authors of publication: Maarten B. Dinger; Michael J. Scott
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 856 - 864
• a: 18.2064 ± 0.0016 Å
• b: 25.301 ± 0.002 Å
• c: 29.814 ± 0.003 Å
• α: 70.109 ± 0.002°
• β: 74.658 ± 0.002°
• γ: 81.012 ± 0.002°
• Cell volume: 12420.8 ± 1.9 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.133
• Residual factor for significantly intense reflections: 0.0892
• Weighted residual factors for significantly intense reflections: 0.2312
• Weighted residual factors for all reflections included in the refinement: 0.2623
• Goodness-of-fit parameter for all reflections included in the refinement: 1.019
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No