Reaction of 2,4,6-Triazido-1,3,5-triazine with Triphenylphosphane. Syntheses and Characterization of the Novel 2-Triphenylphosphanimino-4-azidotetrazolo[5,1-a]-[1,3,5]triazine and 2,4,6-Tris(triphenylphosphanimino)-1,3,5-triazine
Authors of publication
Elmar Kessenich; Kurt Polborn; Axel Schulz
Journal of publication
Inorganic Chemistry
Year of publication
2001
Journal volume
40
Pages of publication
1102 - 1109
a
14.705 ± 0.003 Å
b
17.705 ± 0.004 Å
c
21.528 ± 0.003 Å
α
108.99 ± 0.015°
β
91.612 ± 0.013°
γ
111.66 ± 0.02°
Cell volume
4855 ± 1.9 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.0968
Residual factor for significantly intense reflections
0.0636
Weighted residual factors for all reflections
0.1637
Weighted residual factors for significantly intense reflections
0.1434
Goodness-of-fit parameter for all reflections
1.026
Goodness-of-fit parameter for significantly intense reflections
