Information card for entry 4319465

Structure parameters

• Common name: (Ph4P)(Mn(dca)3)
• Chemical name: tetraphenylphosphonium manganese(II) tris(dicyanamide)
• Formula: C30 H20 Mn N9 P
• Calculated formula: C30 H20 Mn N9 P
• Title of publication: Cation Templation of Anionic Metal Dicyanamide Networks
• Authors of publication: Patricia M. van der Werff; Stuart R. Batten; Paul Jensen; Boujemaa Moubaraki; Keith S. Murray
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 1718 - 1722
• a: 13.2564 ± 0.0003 Å
• b: 7.5742 ± 0.0001 Å
• c: 14.2386 ± 0.0003 Å
• α: 90°
• β: 98.731 ± 0.001°
• γ: 90°
• Cell volume: 1413.08 ± 0.05 ų
• Cell temperature: 123 ± 2 K
• Ambient diffraction temperature: 123 ± 2 K
• Number of distinct elements: 5
• Space group number: 13
• Hermann-Mauguin space group symbol: P 1 2/n 1
• Hall space group symbol: -P 2yac
• Residual factor for all reflections: 0.0359
• Residual factor for significantly intense reflections: 0.0293
• Weighted residual factors for significantly intense reflections: 0.0632
• Weighted residual factors for all reflections included in the refinement: 0.065
• Goodness-of-fit parameter for all reflections included in the refinement: 1.048
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No