Information card for entry 4319571

Structure parameters

• Formula: C21 H22 Cl N4 O8 Re2
• Calculated formula: C21.001 H22 Cl N4 O8 Re2
• Title of publication: Chemistry of Re with N,N'-Bis(2-pyridylmethyl)ethylenediamine (H2pmen): Hydrolysis, Dehydrogenation, and Ternary Complexes
• Authors of publication: Liang Xu; Jason Pierreroy; Brian O. Patrick; Chris Orvig
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 2005 - 2010
• a: 8.4833 ± 0.0002 Å
• b: 18.7387 ± 0.0007 Å
• c: 15.0656 ± 0.0006 Å
• α: 90°
• β: 91.468 ± 0.002°
• γ: 90°
• Cell volume: 2394.13 ± 0.14 ų
• Cell temperature: 173.2 K
• Ambient diffraction temperature: 173.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0507
• Residual factor for significantly intense reflections: 0.027
• Weighted residual factors for all reflections: 0.072
• Weighted residual factors for all reflections included in the refinement: 0.033
• Goodness-of-fit parameter for all reflections: 0.932
• Goodness-of-fit parameter for all reflections included in the refinement: 0.99
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No