Crystallography Open Database

Information card for entry 4319664

4319663 << 4319664 >> 4319665

Preview

Coordinates	4319664.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C121 H154 I N9 O3 Rh
Calculated formula	C121 H154 I N9 O3 Rh
Title of publication	Rh(III) Porphyrins as Building Blocks for Porphyrin Coordination Arrays: From Dimers to Heterometallic Undecamers
Authors of publication	James E. Redman; Neil Feeder; Simon J. Teat; Jeremy K. M. Sanders
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	2486 - 2499
a	11.9139 ± 0.0005 Å
b	16.7586 ± 0.0007 Å
c	28.6361 ± 0.0011 Å
α	104.284 ± 0.001°
β	98.309 ± 0.001°
γ	91.661 ± 0.001°
Cell volume	5470.1 ± 0.4 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0617
Residual factor for significantly intense reflections	0.0467
Weighted residual factors for significantly intense reflections	0.1249
Weighted residual factors for all reflections included in the refinement	0.1303
Goodness-of-fit parameter for all reflections included in the refinement	1.029
Diffraction radiation wavelength	0.6923 Å
Diffraction radiation type	Synchrotron
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4319664.html