Crystallography Open Database

Information card for entry 4319788

4319787 << 4319788 >> 4319789

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Coordinates	4319788.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C84 H101 N12 P3
Calculated formula	C84 H101 N12 P3
Title of publication	Reaction of m-Terphenyldichlorophosphanes with Sodium Azide: Synthesis and Characterization of Stable Azidocyclophosphazenes
Authors of publication	Rudolf J. Wehmschulte; Masood A. Khan; Shawn I. Hossain
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	2756 - 2762
a	11.4044 ± 0.0011 Å
b	13.1141 ± 0.0015 Å
c	27.954 ± 0.003 Å
α	99.744 ± 0.008°
β	91.285 ± 0.008°
γ	102.586 ± 0.008°
Cell volume	4013.8 ± 0.8 Å³
Cell temperature	163 ± 2 K
Ambient diffraction temperature	163 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0991
Residual factor for significantly intense reflections	0.0626
Weighted residual factors for significantly intense reflections	0.1525
Weighted residual factors for all reflections included in the refinement	0.176
Goodness-of-fit parameter for all reflections included in the refinement	1.02
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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