Information card for entry 4319975

Structure parameters

• Formula: C41 H64 Cl2 N6 Ni P2 S2
• Calculated formula: C41 H64 Cl2 N6 Ni P2 S2
• Title of publication: Contrasting Formation of a (Phenylthio)phosphinimine and (Phenylthio)phosphazide. Synthesis of Metal Complexes
• Authors of publication: Luc LePichon; Douglas W. Stephan
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 3827 - 3829
• a: 21.5918 ± 0.0002 Å
• b: 10.6069 ± 0.0001 Å
• c: 22.7952 ± 0.0001 Å
• α: 90°
• β: 106.312 ± 0.001°
• γ: 90°
• Cell volume: 5010.46 ± 0.07 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.1586
• Residual factor for significantly intense reflections: 0.0869
• Weighted residual factors for significantly intense reflections: 0.1957
• Weighted residual factors for all reflections included in the refinement: 0.2303
• Goodness-of-fit parameter for all reflections included in the refinement: 0.968
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No