Information card for entry 4320063

Structure parameters

• Formula: C16 H30 P2 Pd
• Calculated formula: C16 H30 P2 Pd
• Title of publication: Synthesis and Insertion Reactions of the Cyclometalated Palladium-Alkyl Complexes Pd(CH2CMe2-o-C6H4)L2. Observation of a Pentacoordinated Intermediate in the Insertion of SO2
• Authors of publication: J. Cámpora; J. A. López; P. Palma; D. del Rio; E. Carmona; P. Valerga; C. Graiff; A. Tiripicchio
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 4116 - 4126
• a: 9.331 ± 0.003 Å
• b: 16.349 ± 0.001 Å
• c: 12.628 ± 0.003 Å
• α: 90°
• β: 93.9 ± 0.02°
• γ: 90°
• Cell volume: 1922 ± 0.8 ų
• Cell temperature: 290.2 K
• Ambient diffraction temperature: 290.2 K
• Number of distinct elements: 4
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0716
• Weighted residual factors for significantly intense reflections: 0.0864
• Goodness-of-fit parameter for significantly intense reflections: 3.704
• Diffraction radiation wavelength: 1.5418 Å
• Diffraction radiation type: CuKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No