Information card for entry 4320065

Structure parameters

• Formula: C16 H30 O2 P2 Pd S
• Calculated formula: C16 H30 O2 P2 Pd S
• Title of publication: Synthesis and Insertion Reactions of the Cyclometalated Palladium-Alkyl Complexes Pd(CH2CMe2-o-C6H4)L2. Observation of a Pentacoordinated Intermediate in the Insertion of SO2
• Authors of publication: J. Cámpora; J. A. López; P. Palma; D. del Rio; E. Carmona; P. Valerga; C. Graiff; A. Tiripicchio
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 4116 - 4126
• a: 8.244 ± 0.004 Å
• b: 17.519 ± 0.003 Å
• c: 13.854 ± 0.004 Å
• α: 90°
• β: 94.59 ± 0.03°
• γ: 90°
• Cell volume: 1994.5 ± 1.2 ų
• Cell temperature: 290.2 K
• Ambient diffraction temperature: 290.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.0391
• Weighted residual factors for significantly intense reflections: 0.0452
• Goodness-of-fit parameter for significantly intense reflections: 1.367
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No