Information card for entry 4320073

Structure parameters

• Common name: [GeO4Al12(OH)24(H2O)12](SeO4)4.14H2O
• Formula: Al12 Ge H62 O70 Se4
• Calculated formula: Al12 Ge O70 Se4
• Title of publication: Synthesis and Characterization of the GeO4Al12(OH)24(OH2)128+ Polyoxocation
• Authors of publication: Alasdair P. Lee; Brian L. Phillips; Marilyn M. Olmstead; William H. Casey
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 4485 - 4487
• a: 13.0322 ± 0.0007 Å
• b: 13.0322 ± 0.0007 Å
• c: 17.2087 ± 0.0013 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 2922.7 ± 0.3 ų
• Cell temperature: 90 ± 2 K
• Ambient diffraction temperature: 90 ± 2 K
• Number of distinct elements: 5
• Space group number: 119
• Hermann-Mauguin space group symbol: I -4 m 2
• Hall space group symbol: I -4 -2
• Residual factor for all reflections: 0.0648
• Residual factor for significantly intense reflections: 0.0627
• Weighted residual factors for significantly intense reflections: 0.1456
• Weighted residual factors for all reflections included in the refinement: 0.1466
• Goodness-of-fit parameter for all reflections included in the refinement: 1.299
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No