Information card for entry 4320141

Structure parameters

• Formula: C16 H42 Ge9 K4 N6 O4
• Calculated formula: C16 H28 Ge9 K4 N6 O4
• Title of publication: Synthesis and Structure of [K±(2,2)diaza-[18]-crown-6][K3Ge9].2Ethylenediamine: Stabilization of the Two-Dimensional Layer 2\ιnfty[K3Ge91-]
• Authors of publication: Craig Downie; Jiang-Gao Mao; Arnold M. Guloy
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 4721 - 4725
• a: 10.7398 ± 0.0009 Å
• b: 15.8121 ± 0.0013 Å
• c: 12.3259 ± 0.001 Å
• α: 90°
• β: 114.738 ± 0.001°
• γ: 90°
• Cell volume: 1901.1 ± 0.3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.041
• Residual factor for significantly intense reflections: 0.0318
• Weighted residual factors for all reflections: 0.0898
• Weighted residual factors for significantly intense reflections: 0.0842
• Goodness-of-fit parameter for all reflections: 1.024
• Goodness-of-fit parameter for significantly intense reflections: 1.053
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No