Information card for entry 4320224

Structure parameters

• Formula: C188 H120 Hg2 N4 O42 P8 Re14
• Calculated formula: C188 H120 Hg2 N4 O42 P8 Re14
• Title of publication: Synthesis and Characterization of the Dimercury(I)-Linked Compound [PPN]4[(Re7C(CO)21Hg)2]. Oxidative Cleavage of the Mercury-Mercury Bond Leading to Carbidoheptarhenate Complexes of Mercury(II), Including [PPN][Re7C(CO)21Hg(SC(NMe2)2)]
• Authors of publication: Chris A. Wright; Udo Brand; John R. Shapley
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 4896 - 4901
• a: 15.9548 ± 0.0009 Å
• b: 17.3419 ± 0.001 Å
• c: 18.1696 ± 0.0011 Å
• α: 81.939 ± 0.001°
• β: 76.479 ± 0.001°
• γ: 89.014 ± 0.002°
• Cell volume: 4839 ± 0.5 ų
• Cell temperature: 198 ± 2 K
• Ambient diffraction temperature: 198 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1711
• Residual factor for significantly intense reflections: 0.0638
• Weighted residual factors for all reflections: 0.2031
• Weighted residual factors for significantly intense reflections: 0.1405
• Goodness-of-fit parameter for all reflections: 1.039
• Goodness-of-fit parameter for significantly intense reflections: 1.176
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No