Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4320304
Preview
Coordinates | 4320304.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C64 H84 B3 N12 O2.5 Sm |
---|---|
Calculated formula | C67.35 H64 B3 N12 Sm |
Title of publication | Synthesis and Structural Comparison of a Series of Divalent Ln(TpR,R')2 (Ln = Sm, Eu, Yb) and Trivalent Sm(TpMe2)2X (X = F, Cl, I, BPh4) Complexes |
Authors of publication | Anna C. Hillier; XingWang Zhang; Graham H. Maunder; Sung Ying Liu; Todd A. Eberspacher; Mathew V. Metz; Robert McDonald; Ângela Domingos; Noémia Marques; Victor W. Day; Andrea Sella; Josef Takats |
Journal of publication | Inorganic Chemistry |
Year of publication | 2001 |
Journal volume | 40 |
Pages of publication | 5106 - 5116 |
a | 10.045 ± 0.002 Å |
b | 15.411 ± 0.003 Å |
c | 21.047 ± 0.004 Å |
α | 90.93 ± 0.02° |
β | 90.15 ± 0.02° |
γ | 98.46 ± 0.02° |
Cell volume | 3222.2 ± 1.1 Å3 |
Cell temperature | 293 ± 2 K |
Ambient diffraction temperature | 293 ± 2 K |
Number of distinct elements | 6 |
Space group number | 2 |
Hermann-Mauguin space group symbol | P -1 |
Hall space group symbol | -P 1 |
Residual factor for all reflections | 0.11 |
Residual factor for significantly intense reflections | 0.065 |
Weighted residual factors for all reflections | 0.1319 |
Weighted residual factors for significantly intense reflections | 0.1168 |
Goodness-of-fit parameter for all reflections | 0.969 |
Goodness-of-fit parameter for significantly intense reflections | 1.102 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
For the version history of this entry, please navigate to main COD server.
The link is: https://www.crystallography.net/4320304.html
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.