Information card for entry 4320373

Structure parameters

• Formula: C52 H118 Cl0 K N8 O9 Si4 U2
• Calculated formula: C52 H100 K N8 O9 Si4 U2
• Title of publication: Reaction of the Uranyl(VI) Ion (UO22+) with a Triamidoamine Ligand: Preparation and Structural Characterization of a Mixed-Valent Uranium(V/VI) Oxo-Imido Dimer
• Authors of publication: Paul B. Duval; Carol J. Burns; Wayne E. Buschmann; David L. Clark; David E. Morris; Brian L. Scott
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 5491 - 5496
• a: 12.1144 ± 0.0006 Å
• b: 12.6084 ± 0.0006 Å
• c: 14.5072 ± 0.0007 Å
• α: 101.374 ± 0.001°
• β: 103.757 ± 0.001°
• γ: 109.34 ± 0.001°
• Cell volume: 1936.6 ± 0.16 ų
• Cell temperature: 203 ± 2 K
• Ambient diffraction temperature: 203 ± 2 K
• Number of distinct elements: 8
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0524
• Residual factor for significantly intense reflections: 0.0446
• Weighted residual factors for significantly intense reflections: 0.1315
• Weighted residual factors for all reflections included in the refinement: 0.1366
• Goodness-of-fit parameter for all reflections included in the refinement: 1.303
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No