Information card for entry 4320524

Structure parameters

• Formula: C100.8 H77.6 Cl13.6 F16 N12 O16 Rh4
• Calculated formula: C100.8 H64 Cl13.6 F16 N12 O16 Rh4
• Title of publication: Controlling the Dimensionality of Metal-Metal Bonded Rh24+ Polymers by the Length of the Linker. A Disciplined Example of Crystal Engineering
• Authors of publication: F. Albert Cotton; Chun Lin; Carlos A. Murillo
• Journal of publication: Inorganic Chemistry
• Year of publication: 2001
• Journal volume: 40
• Pages of publication: 5886 - 5889
• a: 11.802 ± 0.001 Å
• b: 28.303 ± 0.002 Å
• c: 18.82 ± 0.002 Å
• α: 90°
• β: 95.673 ± 0.002°
• γ: 90°
• Cell volume: 6255.7 ± 1 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 7
• Space group number: 11
• Hermann-Mauguin space group symbol: P 1 21/m 1
• Hall space group symbol: -P 2yb
• Residual factor for all reflections: 0.1807
• Residual factor for significantly intense reflections: 0.0948
• Weighted residual factors for significantly intense reflections: 0.2168
• Weighted residual factors for all reflections included in the refinement: 0.2571
• Goodness-of-fit parameter for all reflections included in the refinement: 1.032
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No