Information card for entry 4320872

Structure parameters

• Formula: F24 Ge20 H69.34 N16 O38.67
• Calculated formula: F24 Ge20 H69.344 N16 O38.672
• Title of publication: Synthesis and Crystal Structure of a Novel Germanate: (NH4)4[(GeO2)3(GeO1.5F3)2].0.67H2O
• Authors of publication: Tony Conradsson; Xiaodong Zou; Mike S. Dadachov
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 1716 - 1720
• a: 7.0065 ± 0.0004 Å
• b: 11.7976 ± 0.0006 Å
• c: 19.52 ± 0.0014 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 1613.52 ± 0.17 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 5
• Space group number: 60
• Hermann-Mauguin space group symbol: P b c n
• Hall space group symbol: -P 2n 2ab
• Residual factor for all reflections: 0.0316
• Residual factor for significantly intense reflections: 0.0223
• Weighted residual factors for significantly intense reflections: 0.0514
• Weighted residual factors for all reflections included in the refinement: 0.0544
• Goodness-of-fit parameter for all reflections included in the refinement: 0.767
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No