Information card for entry 4320905

Structure parameters

• Chemical name: [Nb(NBu-t)Cl2(py){eta2-N(SiMe3)CH2CH2N(H)CH2CH2(SiMe3)2}]
• Formula: C22 H50 Cl2 N5 Nb Si3
• Calculated formula: C22 H50 Cl2 N5 Nb Si3
• Title of publication: Titanium and Niobium Imido Complexes Derived from Diamidoamine Ligands
• Authors of publication: Philip E. Collier; Stephen M. Pugh; Howard S. C. Clark; Jason B. Love; Alexander J. Blake; F. Geoffrey N. Cloke; Philip Mountford
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 2001 - 2005
• a: 9.0658 ± 0.0011 Å
• b: 25.1387 ± 0.0024 Å
• c: 15.1849 ± 0.0015 Å
• α: 90°
• β: 104.989 ± 0.01°
• γ: 90°
• Cell volume: 3342.9 ± 0.6 ų
• Cell temperature: 150 ± 1 K
• Ambient diffraction temperature: 150 ± 1 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0512
• Residual factor for significantly intense reflections: 0.0425
• Weighted residual factors for all reflections: 0.0479
• Weighted residual factors for significantly intense reflections: 0.043
• Goodness-of-fit parameter for all reflections: 1.272
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No