Information card for entry 4320922

Structure parameters

• Formula: C26 H38 Cl2 Cu N4 O10
• Calculated formula: C26 H38 Cl2 Cu N4 O9.95
• Title of publication: Synthesis, X-ray Structure, Single-Crystal EPR and 1H NMR Studies of a Distorted Square Planar Cu(salEen)2(ClO4)2 Complex in a Novel Bilayered Architecture: salEen = N,N-Diethylethylenesalicylidenamine
• Authors of publication: P. S. Subramanian; E. Suresh; D. Srinivas
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 2053 - 2060
• a: 12.055 ± 0.004 Å
• b: 10.652 ± 0.003 Å
• c: 12.701 ± 0.003 Å
• α: 90.54 ± 0.02°
• β: 94.39 ± 0.02°
• γ: 91.35 ± 0.03°
• Cell volume: 1625.6 ± 0.8 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1717
• Residual factor for significantly intense reflections: 0.0889
• Weighted residual factors for significantly intense reflections: 0.22
• Weighted residual factors for all reflections included in the refinement: 0.2438
• Goodness-of-fit parameter for all reflections included in the refinement: 1.017
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No