Crystallography Open Database

Information card for entry 4320935

4320934 << 4320935 >> 4320936

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Coordinates	4320935.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C42 H62 Cl5 Mn N10 O17
Calculated formula	C42 H62 Cl5 Mn N10 O17
Title of publication	Crystal Structures and Magnetic Properties of Metal Complexes Bearing Four Nitronyl Nitroxide Moieties in the Same Coordination Sphere
Authors of publication	Giancarlo Francese; Francisco M. Romero; Antonia Neels; Helen Stoeckli-Evans; Silvio Decurtins
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	2087 - 2095
a	11.5473 ± 0.0008 Å
b	19.2121 ± 0.001 Å
c	25.2361 ± 0.0019 Å
α	90°
β	98.772 ± 0.009°
γ	90°
Cell volume	5533.1 ± 0.6 Å³
Cell temperature	223 ± 2 K
Ambient diffraction temperature	223 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0755
Residual factor for significantly intense reflections	0.0573
Weighted residual factors for significantly intense reflections	0.1721
Weighted residual factors for all reflections included in the refinement	0.1818
Goodness-of-fit parameter for all reflections included in the refinement	1.079
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

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