Information card for entry 4320947

Structure parameters

• Formula: C23 H29 Cl N3 O2.5 P Re
• Calculated formula: C23 H26 Cl N3 O2.5 P Re
• Title of publication: Synthesis and Characterization of Six-Coordinate "3 + 2" Mixed-Ligand Oxorhenium Complexes with theo-Diphenylphosphinophenolato Ligand and Tridentate Coligands of Different N and S Donor Atom Combinations
• Authors of publication: Berthold Nock; Theodosia Maina; Francesco Tisato; Minas Papadopoulos; Catherine P. Raptopoulou; Aris Terzis; Efstratios Chiotellis
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 2178 - 2184
• a: 19.132 ± 0.007 Å
• b: 11.188 ± 0.004 Å
• c: 23.666 ± 0.009 Å
• α: 90°
• β: 98.77 ± 0.01°
• γ: 90°
• Cell volume: 5006 ± 3 ų
• Cell temperature: 298 K
• Ambient diffraction temperature: 298 K
• Number of distinct elements: 7
• Space group number: 15
• Hermann-Mauguin space group symbol: I 1 2/a 1
• Hall space group symbol: -I 2ya
• Residual factor for all reflections: 0.034
• Residual factor for significantly intense reflections: 0.0279
• Weighted residual factors for all reflections: 0.0751
• Weighted residual factors for significantly intense reflections: 0.071
• Goodness-of-fit parameter for all reflections: 1.078
• Goodness-of-fit parameter for significantly intense reflections: 1.083
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No