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Information card for entry 4321002
Preview
Coordinates | 4321002.cif |
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Original paper (by DOI) | HTML |
Formula | C59 H53 Cl4 N P4 Re2 |
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Calculated formula | C59 H53 Cl4 N P4 Re2 |
Title of publication | Reactions of the Dirhenium(II) Complexes Re2X4(μ-dppm)2 (X = Cl, Br; dppm = Ph2PCH2PPh2) with Isocyanides. 21.1A Comparison with the Complexes Re2Cl4(μ-dppE)2 and Re2Cl4(μ-dcpm)2 (dppE = Ph2PC(CH2)PPh2; dcpm = Cy2PCH2PCy2) and the Structural Characterization of Complexes of the Types Re2Cl4(μ-LL)2(CNR), Re2Cl4(μ-LL)2(CNR)2, and [Re2Cl3(μ-LL)2(CNR)3]+ (LL = dppm, dppE, dcpm; R =t-Bu, Xyl) |
Authors of publication | Yan Ding; Shan-Ming Kuang; Michael J. Siwajek; Phillip E. Fanwick; Richard A. Walton |
Journal of publication | Inorganic Chemistry |
Year of publication | 2000 |
Journal volume | 39 |
Pages of publication | 2676 - 2683 |
a | 15.0903 ± 0.0004 Å |
b | 15.0903 ± 0.0004 Å |
c | 26.1521 ± 0.0007 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5955.3 ± 0.3 Å3 |
Cell temperature | 203 ± 2 K |
Number of distinct elements | 6 |
Space group number | 96 |
Hermann-Mauguin space group symbol | P 43 21 2 |
Hall space group symbol | P 4nw 2abw |
Residual factor for significantly intense reflections | 0.0709 |
Weighted residual factors for all reflections included in the refinement | 0.202 |
Goodness-of-fit parameter for all reflections included in the refinement | 1.161 |
Diffraction radiation wavelength | 0.71073 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | No |
Has Fobs | No |
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