Information card for entry 4321170

Structure parameters

• Formula: C37 H40 N12 Ni O7
• Calculated formula: C37 H40 N12 Ni O7
• Title of publication: Synthesis, Characterization, and Spontaneous Resolution of Chiral Nickel(II) Complexes with the Tripod Ligand Tris[2-(((2-phenylimidazol-4-yl)methylidene)amino)ethyl]amine
• Authors of publication: Ikuko Katsuki; Naohide Matsumoto; Masaaki Kojima
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 3350 - 3354
• a: 14.198 ± 0.002 Å
• b: 22.422 ± 0.002 Å
• c: 12.019 ± 0.002 Å
• α: 90°
• β: 90°
• γ: 90°
• Cell volume: 3826.2 ± 0.9 ų
• Cell temperature: 293.2 K
• Ambient diffraction temperature: 293.2 K
• Number of distinct elements: 5
• Space group number: 19
• Hermann-Mauguin space group symbol: P 21 21 21
• Hall space group symbol: P 2ac 2ab
• Residual factor for all reflections: 0.0452
• Residual factor for significantly intense reflections: 0.0452
• Weighted residual factors for significantly intense reflections: 0.0455
• Weighted residual factors for all reflections included in the refinement: 0.0429
• Goodness-of-fit parameter for all reflections included in the refinement: 0.974
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No