Information card for entry 4321172

Structure parameters

• Formula: C50 H58 N10 Ni O10
• Calculated formula: C50 H46 N10 Ni O10
• Title of publication: Synthesis, Characterization, and Spontaneous Resolution of Chiral Nickel(II) Complexes with the Tripod Ligand Tris[2-(((2-phenylimidazol-4-yl)methylidene)amino)ethyl]amine
• Authors of publication: Ikuko Katsuki; Naohide Matsumoto; Masaaki Kojima
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 3350 - 3354
• a: 14.191 ± 0.005 Å
• b: 16.048 ± 0.004 Å
• c: 13.692 ± 0.004 Å
• α: 115.25 ± 0.02°
• β: 111.07 ± 0.03°
• γ: 64.75 ± 0.02°
• Cell volume: 2490 ± 1.4 ų
• Cell temperature: 293.2 K
• Ambient diffraction temperature: 293.2 K
• Number of distinct elements: 5
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0874
• Residual factor for significantly intense reflections: 0.0874
• Weighted residual factors for significantly intense reflections: 0.0862
• Weighted residual factors for all reflections included in the refinement: 0.0862
• Goodness-of-fit parameter for all reflections included in the refinement: 2.615
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No