Information card for entry 4321268

Structure parameters

• Common name: [HB(3,5-(CF3)2Pz)3]AgN3Ad
• Formula: C25 H19 Ag B F18 N9
• Calculated formula: C25 H19 Ag B F18 N9
• Title of publication: Copper and Silver Complexes Containing Organic Azide Ligands: Syntheses, Structures, and Theoretical Investigation of [HB(3,5-(CF3)2Pz)3]CuNNN(1-Ad) and [HB(3,5-(CF3)2Pz)3]AgN(1-Ad)NN (Where Pz = Pyrazolyl and 1-Ad = 1-Adamantyl)
• Authors of publication: H. V. Rasika Dias; Sharon A. Polach; Sor-Koon Goh; Edet F. Archibong; Dennis S. Marynick
• Journal of publication: Inorganic Chemistry
• Year of publication: 2000
• Journal volume: 39
• Pages of publication: 3894 - 3901
• a: 13.2765 ± 0.0016 Å
• b: 13.787 ± 0.0011 Å
• c: 21.479 ± 0.002 Å
• α: 97.805 ± 0.006°
• β: 96.344 ± 0.008°
• γ: 118.5 ± 0.007°
• Cell volume: 3353 ± 0.6 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.0717
• Residual factor for significantly intense reflections: 0.0475
• Weighted residual factors for significantly intense reflections: 0.1104
• Weighted residual factors for all reflections included in the refinement: 0.1238
• Goodness-of-fit parameter for all reflections included in the refinement: 1.011
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No