Synthesis, Characterization, and Coordination Chemistry of a New Geometrically Hindered Trifunctional Ligand, 4,5-Bis(diphenylphosphino)-sym-octahydroacridine N,P,P'-Trioxide
Authors of publication
Gan, Xin-Min; Parveen, Sahrah; Smith, Wayne L.; Duesler, Eileen N.; Paine, Robert T.
Journal of publication
Inorganic Chemistry
Year of publication
2000
Journal volume
39
Journal issue
20
Pages of publication
4591 - 4598
a
13.131 ± 0.002 Å
b
17.579 ± 0.008 Å
c
17.853 ± 0.007 Å
α
90°
β
90°
γ
90°
Cell volume
4121 ± 3 Å3
Cell temperature
293 ± 2 K
Ambient diffraction temperature
293 ± 2 K
Number of distinct elements
6
Space group number
19
Hermann-Mauguin space group symbol
P 21 21 21
Hall space group symbol
P 2ac 2ab
Residual factor for all reflections
0.0853
Residual factor for significantly intense reflections
0.0386
Weighted residual factors for significantly intense reflections
0.075
Weighted residual factors for all reflections included in the refinement
0.0917
Goodness-of-fit parameter for all reflections included in the refinement
