Characterization of the Sterically Encumbered Terphenyl-Substituted Species 2,6-Trip2H3C6S̈n-Sn(Me)2C6H3-2,6-Trip2, an Unsymmetric, Group 14 Element, Methylmethylene, Valence Isomer of an Alkene, Its Related Lithium Derivative 2,6-Trip2H3C6(Me)2Sn-Sn(Li)(Me)C6H3-2,6-Trip2, and the Monomer Sn(t-Bu)C6H3-2,6-Trip2 (Trip = C6H2-2,4,6-i-Pr3)
Authors of publication
Barrett E. Eichler; Philip P. Power
Journal of publication
Inorganic Chemistry
Year of publication
2000
Journal volume
39
Pages of publication
5444 - 5449
a
14.4163 ± 0.0006 Å
b
15.9717 ± 0.0007 Å
c
19.0328 ± 0.0008 Å
α
67.083 ± 0.001°
β
74.633 ± 0.001°
γ
72.654 ± 0.001°
Cell volume
3797.2 ± 0.3 Å3
Cell temperature
90 ± 2 K
Ambient diffraction temperature
90 ± 2 K
Number of distinct elements
4
Space group number
2
Hermann-Mauguin space group symbol
P -1
Hall space group symbol
-P 1
Residual factor for all reflections
0.1149
Residual factor for significantly intense reflections
0.0509
Weighted residual factors for significantly intense reflections
0.1139
Weighted residual factors for all reflections included in the refinement
0.1337
Goodness-of-fit parameter for all reflections included in the refinement
