Information card for entry 4321749

Structure parameters

• Formula: C39 H98.5 Cl Mo2 N12 O2.25 Si6 V
• Calculated formula: C39 H92 Cl Mo2 N12 O2.25 Si6 V
• Title of publication: Heterobimetallic Dinitrogen Complexes That Contain the {[N3N]Mo-NN}- Ligand
• Authors of publication: Myra B. O'Donoghue; William M. Davis; Richard R. Schrock; William M. Reiff
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 243 - 252
• a: 14.1611 ± 0.0001 Å
• b: 21.6122 ± 0.0001 Å
• c: 21.1463 ± 0.0003 Å
• α: 90°
• β: 98.677 ± 0.001°
• γ: 90°
• Cell volume: 6397.8 ± 0.11 ų
• Cell temperature: 183 ± 2 K
• Ambient diffraction temperature: 183 ± 2 K
• Number of distinct elements: 8
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.108
• Residual factor for significantly intense reflections: 0.066
• Weighted residual factors for all reflections: 0.1705
• Weighted residual factors for significantly intense reflections: 0.141
• Goodness-of-fit parameter for all reflections: 1.085
• Goodness-of-fit parameter for significantly intense reflections: 1.165
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No