Information card for entry 4321778

Structure parameters

• Chemical name: magnesium tri(tert-butyl)silylphosphandiide
• Formula: C13 H28 Mg P Si
• Calculated formula: C13 H28 Mg P Si
• Title of publication: Synthesis and Structure of Solvent-Free Hexameric Magnesium Tri(tert-butyl)silylphosphandiide
• Authors of publication: Matthias Westerhausen; Mathias Krofta; Arno Pfitzner
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 598 - 599
• a: 13.594 ± 0.001 Å
• b: 23.177 ± 0.002 Å
• c: 16.351 ± 0.001 Å
• α: 90°
• β: 104.59 ± 0.01°
• γ: 90°
• Cell volume: 4985.6 ± 0.7 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 5
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0896
• Residual factor for significantly intense reflections: 0.0756
• Weighted residual factors for all reflections: 0.2263
• Weighted residual factors for significantly intense reflections: 0.2139
• Goodness-of-fit parameter for all reflections: 1.062
• Goodness-of-fit parameter for significantly intense reflections: 1.122
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No