Information card for entry 4321783

Structure parameters

• Formula: C74 H69 Au3 Cl10 F6 Fe N O6 P3 S3
• Calculated formula: C74 H65 Au3 Cl10 F6 Fe N O6 P3 S3
• Title of publication: Synthesis of the Ferrocene Derivative FcCHN(CH~2~)~2~SH [Fc = (η5-C~5~H~5~)Fe(η5-C~5~H~4~)]: Reactivity toward (Phosphine)gold(I) Cations
• Authors of publication: Eva M. Barranco; M. Concepción Gimeno; Peter G. Jones; Antonio Laguna; M. Dolores Villacampa
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 702 - 706
• a: 60.2 ± 0.006 Å
• b: 14.977 ± 0.002 Å
• c: 19.066 ± 0.003 Å
• α: 90°
• β: 98.367 ± 0.014°
• γ: 90°
• Cell volume: 17007 ± 4 ų
• Cell temperature: 173 ± 2 K
• Ambient diffraction temperature: 173 ± 2 K
• Number of distinct elements: 10
• Space group number: 15
• Hermann-Mauguin space group symbol: C 1 2/c 1
• Hall space group symbol: -C 2yc
• Residual factor for all reflections: 0.1192
• Residual factor for significantly intense reflections: 0.052
• Weighted residual factors for all reflections: 0.105
• Weighted residual factors for significantly intense reflections: 0.0918
• Goodness-of-fit parameter for all reflections: 0.776
• Goodness-of-fit parameter for significantly intense reflections: 0.977
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No