Information card for entry 4321883

Structure parameters

• Formula: C52 H55 N O2 P3 Re
• Calculated formula: C53 H47 N O P3 Re
• Title of publication: Reactions of the Eight-Coordinate Rhenium Complex ReH4(hq)(PPh3)2 (hq = 2-Hydroxyquinoline Monoanion) with Monodentate Tertiary Phosphines: Formation of Pentagonal Bipyramidal Dihydridorhenium(III) Complexes of the Type ReH2(hq)(PPh3)2(PR3)
• Authors of publication: Talia M. McKinney; Phillip E. Fanwick; Richard A. Walton
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 1548 - 1554
• a: 12.24 ± 0.002 Å
• b: 12.411 ± 0.003 Å
• c: 15.196 ± 0.003 Å
• α: 93.196 ± 0.016°
• β: 93.898 ± 0.015°
• γ: 96.215 ± 0.016°
• Cell volume: 2284.9 ± 0.8 ų
• Cell temperature: 296 K
• Ambient diffraction temperature: 296 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.065
• Residual factor for significantly intense reflections: 0.038
• Weighted residual factors for significantly intense reflections: 0.049
• Goodness-of-fit parameter for significantly intense reflections: 1.372
• Diffraction radiation wavelength: 1.54184 Å
• Diffraction radiation type: Cu-Kα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No