Information card for entry 4321900

Structure parameters

• Formula: C23 H49 N Os P2 S
• Calculated formula: C23 H49 N Os P2 S
• Title of publication: Thermally Activated Site Exchange and Quantum Exchange Coupling Processes in Unsymmetrical Trihydride Osmium Compounds
• Authors of publication: Amaya Castillo; Guada Barea; Miguel A. Esteruelas; Fernando J. Lahoz; Agustí LLedós; Feliu Maseras; Javier Modrego; Enrique Oñate; Luis A. Oro; Natividad Ruiz; Eduardo Sola
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 1814 - 1824
• a: 8.832 ± 0.002 Å
• b: 21.124 ± 0.005 Å
• c: 14.923 ± 0.004 Å
• α: 90 ± 0°
• β: 98.23 ± 0.03°
• γ: 90 ± 0°
• Cell volume: 2755.5 ± 1.2 ų
• Cell temperature: 230 ± 0.2 K
• Ambient diffraction temperature: 230 ± 0.2 K
• Number of distinct elements: 6
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for all reflections: 0.0466
• Residual factor for significantly intense reflections: 0.0301
• Weighted residual factors for all reflections: 0.0452
• Weighted residual factors for significantly intense reflections: 0.0328
• Goodness-of-fit parameter for significantly intense reflections: 1.0892
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No