Information card for entry 4321914

Structure parameters

• Formula: C109 H218 Ge18 K6 N13 O36
• Calculated formula: C109 H218 Ge18 K6 N13 O36
• Title of publication: Conformation Isomerism of Nonagermanide Ions. Crystal Structures of Brown and Red [K-([2.2.2]crypt)]6Ge9Ge9.(ethylenediamine)x (x= 0.5, 1.5)
• Authors of publication: Thomas F. Fässler; Uwe Schütz
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 1866 - 1870
• a: 14.397 ± 0.001 Å
• b: 19.765 ± 0.002 Å
• c: 28.898 ± 0.003 Å
• α: 87.485 ± 0.009°
• β: 79.168 ± 0.009°
• γ: 85.415 ± 0.008°
• Cell volume: 8047.3 ± 1.3 ų
• Cell temperature: 213 ± 2 K
• Ambient diffraction temperature: 213 ± 2 K
• Number of distinct elements: 6
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1274
• Residual factor for significantly intense reflections: 0.0745
• Weighted residual factors for significantly intense reflections: 0.1715
• Weighted residual factors for all reflections included in the refinement: 0.2053
• Goodness-of-fit parameter for all reflections included in the refinement: 1.057
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No