Information card for entry 4322022

Structure parameters

• Formula: C36 H56 Al Cl2 N4 P3 Si4
• Calculated formula: C36 H56 Al Cl2 N4 P3 Si4
• Title of publication: Iminophosphine Cycloaddition Reactions of a Diazaphosphoniaaluminatacyclobutane and a Novel Intramolecular Phosphiridine P\ρightarrowP Coordination
• Authors of publication: Neil Burford; Daren J. LeBlanc
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2248 - 2249
• a: 14.6485 ± 0.0003 Å
• b: 18.6224 ± 0.0004 Å
• c: 17.3207 ± 0.0004 Å
• α: 90°
• β: 98.626 ± 0.001°
• γ: 90°
• Cell volume: 4671.47 ± 0.18 ų
• Cell temperature: 150 ± 2 K
• Ambient diffraction temperature: 150 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.0798
• Residual factor for significantly intense reflections: 0.0457
• Weighted residual factors for significantly intense reflections: 0.1212
• Weighted residual factors for all reflections included in the refinement: 0.1361
• Goodness-of-fit parameter for all reflections included in the refinement: 1.022
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No