Information card for entry 4322043

Structure parameters

• Formula: C20 H107 Bi2 Fe2 N5 O92 W20
• Calculated formula: C16 Bi2 Fe2 N4 O93 W20
• Title of publication: Heteropolymetalate Clusters of the Subvalent Main Group Elements BiIII and SbIII
• Authors of publication: Ina Loose; Elisabeth Droste; Michael Bösing; Heinrich Pohlmann; Michael H. Dickman; Cristina Rosu; Michael T. Pope; Bernt Krebs
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2688 - 2694
• a: 13.592 ± 0.005 Å
• b: 19.286 ± 0.005 Å
• c: 21.237 ± 0.005 Å
• α: 90°
• β: 93.09 ± 0.03°
• γ: 90°
• Cell volume: 5559 ± 3 ų
• Cell temperature: 293 ± 2 K
• Ambient diffraction temperature: 293 ± 2 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/n 1
• Hall space group symbol: -P 2yn
• Residual factor for all reflections: 0.1242
• Residual factor for significantly intense reflections: 0.0776
• Weighted residual factors for all reflections: 0.1803
• Weighted residual factors for significantly intense reflections: 0.16
• Goodness-of-fit parameter for all reflections: 1.064
• Goodness-of-fit parameter for significantly intense reflections: 1.158
• Diffraction radiation wavelength: 0.71069 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No