Information card for entry 4322055

Structure parameters

• Formula: C138 H166 B2 Fe2 Ge N12 S6
• Calculated formula: C138 H166 B2 Fe2 Ge N12 S6
• Title of publication: Sn(III) and Ge(III) in the Thiophenolato-Bridged Complexes [LFeSnFeL]n+ and [LFeGeFeL]n+ (n = 2, 3; L = 1,4,7-(4-tert-Butyl-2-mercaptobenzyl)-1,4,7-triazacyclononane)
• Authors of publication: Thorsten Glaser; Eckhard Bill; Thomas Weyhermüller; Wolfram Meyer-Klaucke; Karl Wieghardt
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2632 - 2642
• a: 13.531 ± 0.001 Å
• b: 16.578 ± 0.002 Å
• c: 17.199 ± 0.002 Å
• α: 100.06 ± 0.02°
• β: 112.15 ± 0.02°
• γ: 112.01 ± 0.02°
• Cell volume: 3080.4 ± 1.2 ų
• Cell temperature: 100 ± 2 K
• Ambient diffraction temperature: 100 ± 2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for all reflections: 0.1612
• Residual factor for significantly intense reflections: 0.0792
• Weighted residual factors for all reflections: 0.1896
• Weighted residual factors for significantly intense reflections: 0.1366
• Goodness-of-fit parameter for all reflections: 1.075
• Goodness-of-fit parameter for significantly intense reflections: 1.105
• Diffraction radiation wavelength: 0.71073 Å
• Diffraction radiation type: MoKα
• Has coordinates: Yes
• Has disorder: Yes
• Has Fobs: No