Information card for entry 4322068

Structure parameters

• Formula: C49 H42 Cl3 N3 Os P4 S4
• Calculated formula: C49 H42 Cl3 N3 Os P4 S4
• Title of publication: Reactions of Nitridorhenium(V) and -Osmium(VI) Complexes with Acylating Agents
• Authors of publication: Wa-Hung Leung; Joyce L. C. Chim; Ian D. Williams; Wing-Tak Wong
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 3000 - 3005
• a: 11.475 ± 0.001 Å
• b: 17.493 ± 0.002 Å
• c: 25.697 ± 0.004 Å
• α: 86.12 ± 0.02°
• β: 84.83 ± 0.02°
• γ: 86.85 ± 0.02°
• Cell volume: 5119.3 ± 1.1 ų
• Cell temperature: 298.2 K
• Ambient diffraction temperature: 298.2 K
• Number of distinct elements: 7
• Space group number: 2
• Hermann-Mauguin space group symbol: P -1
• Hall space group symbol: -P 1
• Residual factor for significantly intense reflections: 0.0459
• Weighted residual factors for significantly intense reflections: 0.0465
• Goodness-of-fit parameter for significantly intense reflections: 2.108
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No