Information card for entry 4322073

Structure parameters

• Formula: C33 H49 F3 N O4 Ru2 S3
• Calculated formula: C132 H196 F12 N4 O16 Ru8 S12
• Title of publication: Preparation of Cationic Dinuclear Hydrido Complexes of Ruthenium, Rhodium, and Iridium with Bridging Thiolato Ligands and Their Reactions with Nitrosobenzene
• Authors of publication: Takafumi Iwasa; Hitoshi Shimada; Atsushi Takami; Hiroyuki Matsuzaka; Youichi Ishii; Masanobu Hidai
• Journal of publication: Inorganic Chemistry
• Year of publication: 1999
• Journal volume: 38
• Pages of publication: 2851 - 2859
• a: 14.802 ± 0.003 Å
• b: 12.929 ± 0.004 Å
• c: 19.735 ± 0.003 Å
• α: 90°
• β: 95.48 ± 0.01°
• γ: 90°
• Cell volume: 3759.5 ± 1.5 ų
• Cell temperature: 23 K
• Ambient diffraction temperature: 23 K
• Number of distinct elements: 7
• Space group number: 14
• Hermann-Mauguin space group symbol: P 1 21/c 1
• Hall space group symbol: -P 2ybc
• Residual factor for significantly intense reflections: 0.042
• Weighted residual factors for significantly intense reflections: 0.03
• Goodness-of-fit parameter for significantly intense reflections: 1.53
• Diffraction radiation wavelength: 0.7107 Å
• Diffraction radiation type: MoKalpha
• Has coordinates: Yes
• Has disorder: No
• Has Fobs: No